2-Methyl­sulfonyl-1,2,4-triazolo[1,5-a]quinazolin-5(4H)-one

نویسندگان

  • Rashad Al-Salahi
  • Mohamed Marzouk
  • Mohammed Abbas
  • Seik Weng Ng
چکیده

The triazoloquinazoline fused-ring system of the title compound, C(10)H(8)N(4)O(3)S, is essentially planar (r.m.s. deviation = 0.027 Å). In the crystal, adjacent mol-ecules are linked by N-H⋯O(sulfon-yl) hydrogen bonds, generating a helical chain running along the b axis.

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منابع مشابه

2-Benz­yloxy-1,2,4-triazolo[1,5-a]quinazolin-5(4H)-one. Corrigendum

The name of one of the authors in the paper by Al-Salahi et al. [Acta Cryst. (2011), E67, o1861] is corrected.[This corrects the article DOI: 10.1107/S1600536811024962.].

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Synthesis and pharmacological investigation of novel 4-(3-ethylphenyl)-1-substituted-4H-[1,2,4]triazolo[4,3-a] quinazolin-5-ones as a new class of H1-antihistaminic agents.

A series of novel 4-(3-ethylphenyl)-1-substituted-4H-[1,2,4] triazolo[4,3-a]quinazolin-5-ones (4a-j) were synthesized by the cyclization of 3-(3-ethylphenyl)-2-hydrazino-3H-quinazolin-4-one (3) with various one-carbon donors. The starting material, compound 3, was synthesized from 3-ethyl aniline by a new innovative route with improved yield. When tested for their in vivo H1-antihistaminic acti...

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2-Methyl­sulfanyl-1,2,4-triazolo[1,5-a]quinazolin-5(4H)-one

The non-H atoms of the title compound, C(10)H(8)N(4)OS, lie approximately in a common plane (r.m.s. deviation = 0.058 Å). In the crystal, two mol-ecules are linked across a center of inversion by a pair of N-H⋯N hydrogen bonds, forming a a dimer.

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Synthesis of 1-Substituted-4-(Pyridin-4-yl) [1,2,4] Triazolo [4,3-a] Quinazolin-5(4H)-ones as a New Class of H1- Antihistaminic Agents

Purpose: To synthesize a new series of 1-substituted-4-(pyridin-4-yl) [1,2,4] triazolo[4,3-a]quinazolin5(4H)-ones and evaluate them for H1-antihistaminic activity with negligible side effects in guinea pigs. Methods: The synthesized compounds were characterized by Infrared spectroscopy (IR), proton nuclear magnetic resonance (H-NMR) and mass spectrometry (MS) data. The purity of the compounds w...

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Synthesis, Characterization and Biological Evaluation of Novel 1- Substituted-4-(2-methoxyphenyl)-s-triazolo[4,3-a]quinazolin-5(4H)-ones

In the present study a series of 1-substituted-4-(2-methoxyphenyl)-s-triazolo[4,3-a]quinazolin-5(4H)-ones were synthesized and are screened for their H1-antihistaminic activity. The synthesized compounds were characterized by IR, H-NMR and mass spectral data; the purity of the compounds was determined by elemental analysis. Antihistaminic activity of the title compounds was evaluated by histami...

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عنوان ژورنال:

دوره 68  شماره 

صفحات  -

تاریخ انتشار 2012